D - - L - - L - - 2, 6 - dimethyl-lysyl-phenylalanine amide preparation method of the tyrosyl - L -

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The invention relates to a process for solution-phase synthesis of D-Arginyl-2, 6-dimethyl-L-tyrosyl-L-lysyl-L-phenylalaninamide, an active ingredient used for both common and rare diseases including a mitochondrial targeted therapy for ischemia reperfusion injury.