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METHOD FOR ISOLATING RARE EARTHS AND/OR ELEMENT (S) (S) ADDITIONAL METAL (S) CONTAINED IN THE MAGNET

2025-06-18 01:304080下载
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A isolating method including : (i) arranging material forming a magnetic phase as a demagnetised powder, having an average particle size no larger than 700 μm without particles not making up the magnetic phase; (ii) dissolving the powder of step (i) in an acid medium with at least one oxidising agent in the presence of hydroxide ions, at a pH strictly lower than 7; (iii) precipitating the adjacent metal element(s) in the hydroxide state by adding to the solution obtained at the end of step (ii) an effective amount of hydroxylated base; (iv) isolating the metal hydroxide precipitate formed at the end of step (iii) and, when necessary, recovering same; (v) precipitating the rare earth elements in the oxalate state in the solution without adjacent metal element(s) and obtained at the end of step (iv); and (vi) recovering the rare earths in the precipitated state of rare earth oxalate.


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