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The present invention relates to a quantitative analysis method of a metal composition and a content of a catalyst dissolved in organic solvents. The quantitative analysis method of the present invention does not involve decomposition by acid and ashing at a high temperature as preprocess of a catalyst sample, does not use a glass vial, remarkably shortens quantitative analysis time of the catalyst, and can measure the exact content of the catalyst since impurities other than the catalyst are not measured.(AA) Pd peak comparison (NMP vs DI)COPYRIGHT KIPO 2019