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METHOD FOR PROCESSING FLUORINE-CONTAINING RARE EARTH MINERAL PARTICLES 发明授权

2023-02-22 4190 227K 0

专利信息

申请日期 2025-06-28 申请号 EP19823875
公开(公告)号 EP3663421B1 公开(公告)日 2022-01-12
公开国别 EP 申请人省市代码 全国
申请人 Baotou Research Institute of Rare Earths; National Engineering Research Centre of Ruike Rare Earth Metallurgy and Function Materials Co Ltd
简介 The present disclosure discloses a method for treating fluorine-containing rare earth mineral particles, comprising the following steps : (1) mixing the first batch of fluorine-containing rare earth mineral particles with the first sulfuric acid solution according to the weight ratio of 2-10 : 1 of the sulfuric acid in the first sulfuric acid solution to the first batch of fluorine-containing rare earth mineral particles, and then heating the mixture for liquid-solid reaction, condensing and absorbing steam through a tail gas system, wherein a sulfuric acid concentration of the first sulfuric acid solution is 40-85wt%; (2) after the reaction, separating solid phase and liquid phase to obtain acid filtrate and acid residue; (3) leaching the acid residue with water to obtain aqueous leaching liquor of rare earth sulfate and aqueous leaching residue; (4) adding the second sulfuric acid solution to the acid filtrate so that the sulfuric acid concentration of the acid filtrate is 40-85wt%; and then circularly executing the steps (1) - (3) for treating the ithbatch of fluorine-containing rare earth mineral particles, wherein the character "i" is a natural number greater than or equal to 2.. The method of the present disclosure realizes the rapid decomposition of the fluorine-containing rare earth mineral particles. In addition, the reaction is easy to be controlled, and the residual acid resources can be recycled.


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