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Method for synthesizing rare earth metal extractant 发明授权

2023-07-31 1250 954K 0

专利信息

申请日期 2025-06-24 申请号 US13808220
公开(公告)号 US9133100B2 公开(公告)日 2015-09-15
公开国别 US 申请人省市代码 全国
申请人 Kazuaki Sakaki; Hiroto Sugahara; Tetsuya Kume; Masaki Ohashi; Hirochika Naganawa; Kojiro Shimojo
简介 A rare earth metal extractant containing, as the extractant component, dialkyldiglycol amide acid which is excellent in breaking down light rare earth elements is reacted in diglycolic acid (X mol) and an esterification agent (Y mol) at a reaction temperature of 70° C. or more and for a reaction time of one hour or more such that the mol ratio of Y/X is 2.5 or more, and is subjected to vacuum concentration. Subsequently, a reaction intermediate product is obtained by removing unreacted products and reaction residue. Then a nonpolar or low-polar solvent which is an organic solvent for forming an organic phase during solvent extraction of the rare earth metal and which is capable of dissolving dialkyldiglycol amide acid is added as the reaction solvent, and the reaction intermediate product is reacted with dialkyl amine (Z mol) such that the mol ratio of Z/X is 0.9 or more.


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