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METHOD FOR PREPARING HIGH-PERFORMANCE RARE EARTH-IRON-COBALT SILICIDE COMPOUND WITH NAZN13 STRUCTURE 发明申请

2023-10-27 1210 836K 0

专利信息

申请日期 2025-06-27 申请号 WOCN11079874
公开(公告)号 WO2012041171A1 公开(公告)日 2012-04-05
公开国别 WO 申请人省市代码 全国
申请人 UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING; LONG Yi; LI Xiaolan; WANG Han; YE Rongchang; CHANG Yongqin; WAN Farong
简介 Provided is a method for the preparation of a high-performance rare earth-iron-cobalt silicide compound having a NaZn13 structure and belonging to the field of materials processing. Specifically, the invention concerns a powder with a granularity of 1μm to 40μm of a master alloy comprising iron-cobalt silicide and a rare earth consisting of main-phase and impurity-phase rare earths in a 1 : 13 proportion, the powder being placed in a mold, and the mold placed in a plasma for low-temperature short sintering, the temperature whereof ranging between 600°C and 1100°C and the time between 2 and 10 minutes. The sintering produces a rare earth-iron-cobalt silicide compound having a NaZn13 structure. The present invention allows preparation of large pieces of a rare earth-iron-cobalt silicide compound having a flexural strength in excess of 110 Mpa, able to withstand pressure in excess of 100N and having even Curie temperature distribution. For use in magnetic refrigeration technology and materials using a rare earth-iron-cobalt silicide compound having a NaZn13 structure.


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