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Synthesizing 3, 5-dichloro-anisole comprises reacting trichloro-benzene and methanolate of alkaline 发明申请

2023-07-19 1430 125K 0

专利信息

申请日期 2025-07-18 申请号 FR10050232
公开(公告)号 FR2950882A1 公开(公告)日 2011-04-08
公开国别 FR 申请人省市代码 全国
申请人 COMMISSARIAT ENERGIE ATOMIQUE
简介 The invention relates to a method for the synthesis of 3, 5- dichloroanisole from the 1, 3, 5-trichlorobenzene, which comprises : a) the reaction of 1, 3, 5-trichlorobenzene and a methanolate of an alkali metal or alkaline-earth metal in a first solvent, aprotic polar; b) the precipitation of the product resulting from step a) in a second solvent; and c) collecting the resulting precipitate; and wherein the first and second solvents are not part substances regarded as carcinogenic, mutagenic and reprotoxic Regulations/or by the (EC) No. 1272/2008 of the European Parliament and of the Council of 16 December 2008. Application : synthesis of 1, 3, 5-triamino -2, 4, 6-trinitrobenzene, the 3, 5- dichloroanisole is an intermediate product.


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