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METHOD OF REGENERATING THERMOSET EPOXY RESIN AND COMPOSITION FOR REGENERATION OF THERMOSET RESIN 发明申请

2023-03-31 2430 1275K 0

专利信息

申请日期 2025-06-24 申请号 WOJP09068352
公开(公告)号 WO2010050442A1 公开(公告)日 2010-05-06
公开国别 WO 申请人省市代码 全国
申请人 NATIONAL UNIVERSITY CORPORATION SHIZUOKA UNIVERSITY; OKAJIMA Idzumi; SAKO Takeshi
简介 A method comprising : a step in which a resinous structure comprising a thermoset epoxy resin having ester bonds and at least one member selected from inorganic fibers and an inorganic filler is treated with a supercritical or subcritical alcohol in the absence of any catalyst to selectively cleave the ester bonds of the thermoset epoxy resin and thereby decompose the thermoset epoxy resin; a step in which the decomposition products are separated into liquid matter and the inorganic fibers and/or inorganic filler; a step in which the alcohol is removed from the separated liquid matter to recover a decomposed epoxy resin; and a step in which the decomposed epoxy resin recovered is reacted with a hardener to produce a re-cured resin, the hardener being used in an amount of 25-55 mass% relative to the sum of the decomposed epoxy resin and the hardener.  By this method, a thermoset epoxy resin can be decomposed at a relatively low temperature into components which can be cured again.  A re-cured resin equal or superior in strength to the original thermoset epoxy resin is obtained.


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