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Continuous synthetic process of phosphor in supercritical water and apparatus being used therein 发明申请

2022-12-24 5300 327K 0

专利信息

申请日期 2025-06-30 申请号 KR1020040092028
公开(公告)号 KR1020060044194A 公开(公告)日 2006-05-16
公开国别 KR 申请人省市代码 全国
申请人 KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCES(KIGAM); YONSEI UNIVERSITY
简介 PURPOSE : Provided are a method for preparing a phosphor having uniform size and shape under supercritical water condition within a short time, a phosphor prepared by the method, and its apparatus. CONSTITUTION : The method comprises the steps of mixing a water-soluble metal solution containing a host and an activator and an alkali solution to prepare a hydroxide salt solution; mixing the hydroxide salt solution and preheated water to maintain the temperature of the reaction mixture to be 150-200 deg.C; injecting the reaction mixture into a main reactor maintained in supercritical water state to prepare a phosphor particle; and condensing, filtering and drying the phosphor particle. Preferably the host is yttrium or aluminum; and the activator is a rare earth metal. © KIPO 2006


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