Among HDDR, hydrogen release and re-coupling stage and a control method, including hydrogen releas

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The present invention features a method for controlling a hydrogen desorption-recombination step in a HDDR process in which the hydrogen release rate is controlled such that the time necessary for an endothermic reaction in the hydrogen desorption-recombination step in the hydrogenation-disproportionation-desorption-recombination (HDDR) process exceeds three minutes.